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Gilabert, J. y Vinas, P.",
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Gilabert, J. y Vinas, P.",
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Gilabert, J. y Vinas, P."
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  "notes": "The use of dispersive liquid-liquid microextraction 
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  "notes": "The use of dispersive liquid-liquid microextraction 
            
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(DLLME) is proposed for the preconcentration of thirteen lipophilic 
96
(DLLME) is proposed for the preconcentration of thirteen lipophilic 
            
97
marine toxins in seawater samples. For this purpose, 0.5 mL of 
97
marine toxins in seawater samples. For this purpose, 0.5 mL of 
            
98
methanol and 440 mu L of chloroform were injected into 12 mL of 
98
methanol and 440 mu L of chloroform were injected into 12 mL of 
            
99
sample. The enriched organic phase, once evaporated and reconstituted 
99
sample. The enriched organic phase, once evaporated and reconstituted 
            
100
in methanol, was analyzed by reversed-phase liquid chromatography with 
100
in methanol, was analyzed by reversed-phase liquid chromatography with 
            
101
triple-quadrupole tandem mass spectrometry. A central composite design 
101
triple-quadrupole tandem mass spectrometry. A central composite design 
            
102
multivariate method was used to optimize the interrelated parameters 
102
multivariate method was used to optimize the interrelated parameters 
            
103
affecting DLLME efficiency. The absence of any matrix effect in the 
103
affecting DLLME efficiency. The absence of any matrix effect in the 
            
104
samples allowed them to be quantified against aqueous standards. The 
104
samples allowed them to be quantified against aqueous standards. The 
            
105
optimized procedure was validated by recovery studies, which provided 
105
optimized procedure was validated by recovery studies, which provided 
            
106
values in the 82-123% range. The detection limits varied between 0.2 
106
values in the 82-123% range. The detection limits varied between 0.2 
            
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and 5.7 ng L-1, depending on the analyte, and the intraday precision 
107
and 5.7 ng L-1, depending on the analyte, and the intraday precision 
            
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values were in the 0.1-7.5% range in terms of relative standard 
108
values were in the 0.1-7.5% range in terms of relative standard 
            
109
deviation. Ten water samples taken from different points of the Mar 
109
deviation. Ten water samples taken from different points of the Mar 
            
110
Menor lagoon were analyzed and were found to be free of the studied 
110
Menor lagoon were analyzed and were found to be free of the studied 
            
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toxins.",
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toxins.",
            
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    "es": "The use of dispersive liquid-liquid microextraction (DLLME) 
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    "es": "The use of dispersive liquid-liquid microextraction (DLLME) 
            
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is proposed for the preconcentration of thirteen lipophilic marine 
114
is proposed for the preconcentration of thirteen lipophilic marine 
            
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toxins in seawater samples. For this purpose, 0.5 mL of methanol and 
115
toxins in seawater samples. For this purpose, 0.5 mL of methanol and 
            
116
440 mu L of chloroform were injected into 12 mL of sample. The 
116
440 mu L of chloroform were injected into 12 mL of sample. The 
            
117
enriched organic phase, once evaporated and reconstituted in methanol, 
117
enriched organic phase, once evaporated and reconstituted in methanol, 
            
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was analyzed by reversed-phase liquid chromatography with 
118
was analyzed by reversed-phase liquid chromatography with 
            
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triple-quadrupole tandem mass spectrometry. A central composite design 
119
triple-quadrupole tandem mass spectrometry. A central composite design 
            
120
multivariate method was used to optimize the interrelated parameters 
120
multivariate method was used to optimize the interrelated parameters 
            
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affecting DLLME efficiency. The absence of any matrix effect in the 
121
affecting DLLME efficiency. The absence of any matrix effect in the 
            
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samples allowed them to be quantified against aqueous standards. The 
122
samples allowed them to be quantified against aqueous standards. The 
            
123
optimized procedure was validated by recovery studies, which provided 
123
optimized procedure was validated by recovery studies, which provided 
            
124
values in the 82-123% range. The detection limits varied between 0.2 
124
values in the 82-123% range. The detection limits varied between 0.2 
            
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and 5.7 ng L-1, depending on the analyte, and the intraday precision 
125
and 5.7 ng L-1, depending on the analyte, and the intraday precision 
            
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values were in the 0.1-7.5% range in terms of relative standard 
126
values were in the 0.1-7.5% range in terms of relative standard 
            
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deviation. Ten water samples taken from different points of the Mar 
127
deviation. Ten water samples taken from different points of the Mar 
            
128
Menor lagoon were analyzed and were found to be free of the studied 
128
Menor lagoon were analyzed and were found to be free of the studied 
            
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toxins."
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toxins."
            
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Liquid-Liquid Microextraction and Liquid Chromatography with Triple 
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Quadrupole Mass Spectrometry",
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    "es": "Monitoring Lipophilic Toxins in Seawater Using Dispersive 
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Liquid-Liquid Microextraction and Liquid Chromatography with Triple 
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Liquid-Liquid Microextraction and Liquid Chromatography with Triple 
            
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Quadrupole Mass Spectrometry"
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