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  "name": "dd7326be-c55f-577e-b5ca-f55df15d299b",
            
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  "notes": "The use of dispersive liquid-liquid microextraction 
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  "notes": "The use of dispersive liquid-liquid microextraction 
            
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(DLLME) is proposed for the preconcentration of thirteen lipophilic 
106
(DLLME) is proposed for the preconcentration of thirteen lipophilic 
            
97
marine toxins in seawater samples. For this purpose, 0.5 mL of 
107
marine toxins in seawater samples. For this purpose, 0.5 mL of 
            
98
methanol and 440 mu L of chloroform were injected into 12 mL of 
108
methanol and 440 mu L of chloroform were injected into 12 mL of 
            
99
sample. The enriched organic phase, once evaporated and reconstituted 
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sample. The enriched organic phase, once evaporated and reconstituted 
            
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in methanol, was analyzed by reversed-phase liquid chromatography with 
110
in methanol, was analyzed by reversed-phase liquid chromatography with 
            
101
triple-quadrupole tandem mass spectrometry. A central composite design 
111
triple-quadrupole tandem mass spectrometry. A central composite design 
            
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multivariate method was used to optimize the interrelated parameters 
112
multivariate method was used to optimize the interrelated parameters 
            
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affecting DLLME efficiency. The absence of any matrix effect in the 
113
affecting DLLME efficiency. The absence of any matrix effect in the 
            
104
samples allowed them to be quantified against aqueous standards. The 
114
samples allowed them to be quantified against aqueous standards. The 
            
105
optimized procedure was validated by recovery studies, which provided 
115
optimized procedure was validated by recovery studies, which provided 
            
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values in the 82-123% range. The detection limits varied between 0.2 
116
values in the 82-123% range. The detection limits varied between 0.2 
            
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and 5.7 ng L-1, depending on the analyte, and the intraday precision 
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and 5.7 ng L-1, depending on the analyte, and the intraday precision 
            
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values were in the 0.1-7.5% range in terms of relative standard 
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values were in the 0.1-7.5% range in terms of relative standard 
            
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deviation. Ten water samples taken from different points of the Mar 
119
deviation. Ten water samples taken from different points of the Mar 
            
110
Menor lagoon were analyzed and were found to be free of the studied 
120
Menor lagoon were analyzed and were found to be free of the studied 
            
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toxins.",
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toxins.",
            
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    "es": "The use of dispersive liquid-liquid microextraction (DLLME) 
            
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is proposed for the preconcentration of thirteen lipophilic marine 
            
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toxins in seawater samples. For this purpose, 0.5 mL of methanol and 
125
toxins in seawater samples. For this purpose, 0.5 mL of methanol and 
            
116
440 mu L of chloroform were injected into 12 mL of sample. The 
126
440 mu L of chloroform were injected into 12 mL of sample. The 
            
117
enriched organic phase, once evaporated and reconstituted in methanol, 
127
enriched organic phase, once evaporated and reconstituted in methanol, 
            
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was analyzed by reversed-phase liquid chromatography with 
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was analyzed by reversed-phase liquid chromatography with 
            
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triple-quadrupole tandem mass spectrometry. A central composite design 
129
triple-quadrupole tandem mass spectrometry. A central composite design 
            
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multivariate method was used to optimize the interrelated parameters 
130
multivariate method was used to optimize the interrelated parameters 
            
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affecting DLLME efficiency. The absence of any matrix effect in the 
131
affecting DLLME efficiency. The absence of any matrix effect in the 
            
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samples allowed them to be quantified against aqueous standards. The 
132
samples allowed them to be quantified against aqueous standards. The 
            
123
optimized procedure was validated by recovery studies, which provided 
133
optimized procedure was validated by recovery studies, which provided 
            
124
values in the 82-123% range. The detection limits varied between 0.2 
134
values in the 82-123% range. The detection limits varied between 0.2 
            
125
and 5.7 ng L-1, depending on the analyte, and the intraday precision 
135
and 5.7 ng L-1, depending on the analyte, and the intraday precision 
            
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values were in the 0.1-7.5% range in terms of relative standard 
136
values were in the 0.1-7.5% range in terms of relative standard 
            
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deviation. Ten water samples taken from different points of the Mar 
137
deviation. Ten water samples taken from different points of the Mar 
            
128
Menor lagoon were analyzed and were found to be free of the studied 
138
Menor lagoon were analyzed and were found to be free of the studied 
            
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toxins."
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toxins."
            
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